Friedel-Crafts Acylation. This electrophilic aromatic substitution allows the synthesis of monoacylated products from the reaction between arenes and acyl chlorides or anhydrides. The products are deactivated, and do not undergo a second substitution. Normally, a stoichiometric amount of the Lewis acid catalyst is required. exothermic reactions and quenches (Friedel–Crafts acylation conducted under neat conditions and at elevated temperature and oxidative 1,2-aryl shift) were mitigated through a funda- mental advantage of continuous flow over batch synthesis; only a small amount of material relative to the output of the.
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Aside from the high throughput, several other aspects of this synthesis expand the capabilities of continuous-flow processing, including a Friedel–Crafts acylation run under neat conditions and promoted by AlCl3, an exothermic in-line quench of high concentrations of precipitation-prone AlCl3, liquid–liquid. Organic synthesis. ○ A) The original Boots synthesis of ibuprofen. Step1. Friedel-Crafts acetylation of 2-methylpropylbenzene. Step2. Reaction with ethyl chloroacetate. (Darzens reaction) gave the α,β-epoxy ester.
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